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2-Bromo-5-methoxybenzyl bromide

2-Bromo-5-methoxybenzyl bromide structure

CAS No:
19614-12-1
Formula:
C8H8Br2O
Chemical Name:
2-Bromo-5-methoxybenzyl bromide
Synonyms:
Benzene,1-bromo-2-(bromomethyl)-4-methoxy-;Anisole,4-bromo-3-(bromomethyl)-;1-Bromo-2-(bromomethyl)-4-methoxybenzene;2-Bromo-5-methoxybenzyl bromide;4-Bromo-3-(bromomethyl)-1-methoxybenzene;5-Methoxy-2-bromobenzyl bromide;3-Methoxy-6-bromobenzyl bromide
Categories:
Pharmaceutical Intermediates > Bulk Drug Intermediates

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2-Bromo-5-methoxybenzyl bromide Basic Attributes

Molecular Weight：

279.958

Exact Mass：

279.96

DSSTox ID：

DTXSID90393317

HScode：

2909309090

Characteristics

PSA：

9.2

XLogP3：

3.1

Appearance：

White to beige Solid

Density：

1.8±0.1 g/cm3

Melting Point：

85-87 °C

Boiling Point：

299.6°C at 760 mmHg

Flash Point：

120.3±21.7 °C

Refractive Index：

1.584

Water Solubility：

soluble in hot methanol. Slightly soluble in water.

Vapor Pressure：

0.0021mmHg at 25°C

Safety Information

Hazard category：

Transport codes：

UN 3261 8/PG 2

wgk germany：

hazard class code：

safety instructions：

26-36/37/39-45

Marks：

Precautionary statement(s)：

P280-P305 + P351 + P338-P310

Hazard Statements：

H314

GHS Classification：

|Danger|H314 (100%): Causes severe skin burns and eye damage [Danger Skin corrosion/irritation]|P260, P264, P280, P301+P330+P331, P303+P361+P353, P304+P340, P305+P351+P338, P310, P321, P363, P405, and P501|Aggregated GHS information provided by 42 companies from 4 notifications to the ECHA C&L Inventory.

2-Bromo-5-methoxybenzyl bromide Use and Manufacturing

To a CCl4 solution (125 mL) of 2-bromo-5-methoxytoluene (0.050 mol) and NBS (0.055 mol) was added AIBN (0.001 mol), and the mixture was stirred at 80 °C for 18 h. The mixture was diluted with hexane before filtration through a Celite pad. Evaporation of the solvent followed by washing of the residue with ethyl acetate gave 4-bromo-3-(bromomethyl)anisole.a a a l-Bromo-2-(bromomethyl)-4-methoxybenzeneTo a solution of 173 g (0.86 mol) of l-bromo-4-methoxy-2-methylbenzene in 850 ml of CCI1-Bromo-2-(bromomethyl)-4-methoxybenzene 1-Bromo-2-(bromomethyl)-4-methoxybenzene A dry, stir bar-equipped, 3-neck 250 mL round bottom flask was fitted with a reflux condenser and put under nitrogen. 77 1-bromo-4-methoxy-2-methylbenzene (1.39 mL, 2.011 g, 10.0 mmol, 1.00 eq), 121 CClInto a 1000-mL round-bottom flask, was placed a solution of l-bromo-4-methoxy- 2-methylbenzene (20 g, 100.00 mmol, 1.00 equiv) in CCI1-Bromo-2-(bromomethyl)-4-methoxybenzene 1-Bromo-2-(bromomethyl)-4-methoxybenzene 1-2)

Computed Properties

Molecular Weight:279.96
XLogP3:3.1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:279.89214
Monoisotopic Mass:277.89419
Topological Polar Surface Area:9.2
Heavy Atom Count:11
Complexity:119
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Recommended Suppliers of 2-Bromo-5-methoxybenzyl bromide

HANGZHOU LEAP CHEM CO., LTD. Contact Supplier

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2-Bromo-5-methoxybenzyl bromide

CAS No.: 19614-12-1

Content: 99.00%

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Tianjin Jinshu Technology Co., Ltd. Contact Supplier

CN
2 YRS

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Trader Supplier of peptone

High purity 2-Bromo-5-methoxybenzyl bromide human with Safe Delivery

CAS No.: 19614-12-1

Grade: Industrial Grade

Content: 99%

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Guide of 2-Bromo-5-methoxybenzyl bromide

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Recommended Suppliers
Latest News
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2-Bromo-5-methoxybenzyl bromide

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