N-(2-Phenylacetyl)guanosine
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N-(2-Phenylacetyl)guanosine
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CAS No:
132628-16-1
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Formula:
C18H19N5O6
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Chemical Name:
N-(2-Phenylacetyl)guanosine
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Synonyms:
Guanosine,N-(2-phenylacetyl)-;Guanosine,N-(phenylacetyl)-;N-(2-Phenylacetyl)guanosine
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CAS No:
N-(2-Phenylacetyl)guanosine Use and Manufacturing
Another take a flask, Add 1200 g of water, Water temperature 15_20 C, Stir, The reaction system of intermediate 1Pi was slowly added to the water, Feeding process temperature control 20-30 C, After the addition, keep the reaction at 20-30 C for 5 hours.After completion of the reaction, the temperature of the system was raised to 70-75 C and concentrated in vacuo.The remaining amount of solvent is not higher than the total amount of 15%After completion of the concentration, add 1300 kg of distilled water to the system to reduce the temperature of the system to 20-25 C for 2 hours, Precipitation of crystals, Filtration to obtain a crude solid. The crude product was added to the flask, 80 g of methanol was added, 500 g of ethyl acetate solvent, Stirred at room temperature for 2 hours, filter, Washed with 80 g of ethyl acetate, Dried at 30-35 C for 4 hours in vacuo to give 139 g of N2-phenylacetyl-D-guanosine product, White solid powder, yield 98.09%, purity 99.21%.
Computed Properties
Molecular Weight:401.4
XLogP3:-0.1
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:5
Exact Mass:401.13353334
Monoisotopic Mass:401.13353334
Topological Polar Surface Area:158
Heavy Atom Count:29
Complexity:669
Defined Atom Stereocenter Count:4
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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