N-FMOC-D-glutamic acid
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N-FMOC-D-glutamic acid
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CAS No:
104091-09-0
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Formula:
C20H19NO6
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Chemical Name:
N-FMOC-D-glutamic acid
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Synonyms:
D-Glutamic acid,N-[(9H-fluoren-9-ylmethoxy)carbonyl]-;N-[(9H-Fluoren-9-ylmethoxy)carbonyl]-D-glutamic acid;N-FMOC-D-glutamic acid;D-Fmoc-glutamic acid;(2R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)pentanedioic acid;(2R)-2-([[(9H-Fluoren-9-yl)methoxy]carbonyl]amino)pentanedioic acid
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CAS No:
Characteristics
113
2.5
1.366±0.06 g/cm3(Predicted)
635.8±50.0 °C(Predicted)
338.3±30.1 °C
19 ° (C=1, DMF)
N-FMOC-D-glutamic acid Use and Manufacturing
General procedure: To a solution of H-Phe-OH (100 mg, 60.5 mmol) in 50 percent MeCN (6.1 mL)were added Fmoc-OPhth (233 mg, 60.5 mmol) and K2CO3 (167 mg, 121 mmol) and stirred at room temperature. After 2 h of stirring saturated sodium bicarbonate solution and H2O were added and the resulting solution was washed with diethyl ether. The aqueous phase is acidified to pH 1 with 1M HCl and extracted with diethyl ether. The organic phase was washed with 1 M HCl, H2O, brine, dried over MgSO4. The filtrate was evaporatedevaporated under reduced pressure to give yellow solid as crude product.
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