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BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE

BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE structure

CAS No:
310454-53-6
Formula:
C16H21NO4
Chemical Name:
BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE
Synonyms:
CBZ-PIPERIDINE-3-CARBOXYLIC ACID ETHYL ESTER;BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE;Benzyl ethyl piperidine-1,3-dicarboxylate 97%;1-Benzyl 3-ethyl piperidine-1,3-dicarboxylate;1,3-Piperidinedicarboxylic acid, 3-ethyl 1-(phenylMethyl) ester;1-Cbz-piperidine-3-carboxylic acid ethyl ester;1-O-benzyl 3-O-ethyl piperidine-1,3-dicarboxylate

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BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE Basic Attributes

Molecular Weight：

291.34

Exact Mass：

291.147064

Characteristics

PSA：

55.8

XLogP3：

2.3

Density：

1.2±0.1 g/cm3

Boiling Point：

537.4°C at 760 mmHg

Flash Point：

198.0±28.7 °C

Refractive Index：

1.534

Safety Information

Marks：

Precautionary statement(s)：

P261, P264, P271, P280, P302+P352, P304+P340, P305+P351+P338, P312, P321, P332+P313, P337+P313, P362, P403+P233, P405, P501

Hazard Statements：

H315

BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE Use and Manufacturing

Step 1: [00248] Step A: To ethyl piperidine-3 -carboxylate (5.0 g, 30.2 mmol) and KTo a solution of ethyl piperidine-3-carboxylate (4 g, 25.4 mmol) in THF (30 mL) and water (30.0 mL) was added a2C03 (6.74 g, 63.6 mmol). The resulting suspension was stirred at rt for 20 min. After this time, benzyl carbonochloridate (4.12 g, 24.17 mmol) was added dropwise. After addition, the stirring solution became milky, and a white precipitate formed. After stirring at rt for 2h, the reaction was partitioned between EtOAc and water. The separated aqueous phase was extracted with EtOAc (2x). The combined organics were washed with water and saturated aqueous NaCl. The organic layer was dried over NaStep 1. 1-Benzyl 3-ethyl piperidine-1, 3-dicarboxylate; A 250-mL round-bottomed flask was charged with a solution of NaHCO

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Cbz-Piperidine-3-carboxylic acid ethyl ester

CAS No.: 310454-53-6

Content: 99.00%

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Guide of BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
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BENZYL ETHYL PIPERIDINE-1,3-DICARBOXYLATE

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