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Pigment Yellow 65

Pigment Yellow 65 structure

Pigment Yellow 65 

structure
  • CAS No:

    6528-34-3

  • Formula:

    C18H18N4O6

  • Chemical Name:

    Pigment Yellow 65

  • Synonyms:

    Butanamide,2-[2-(4-methoxy-2-nitrophenyl)diazenyl]-N-(2-methoxyphenyl)-3-oxo-;Butanamide,2-[(4-methoxy-2-nitrophenyl)azo]-N-(2-methoxyphenyl)-3-oxo-;2-[2-(4-Methoxy-2-nitrophenyl)diazenyl]-N-(2-methoxyphenyl)-3-oxobutanamide;C.I. Pigment Yellow 65;C.I. 11740;Hansa Yellow 3RN;Hansa Yellow RN;Permansa Yellow Lightfast Medium RA 12187;Acetanil Yellow RTCA;Dalamar Yellow YT-820-D;Dalamar Yellow YT 820D;Pigment Yellow 65;Sunbrite Yellow 65;Permanent Yellow RN;2-[2-(4-Methoxy-2-nitrophenyl)diazen-1-yl]-N-(2-methoxyphenyl)-3-oxobutanamide;57769-74-1

  • Categories:

    Dyes and Pigments  >  Pigment

Description

DryPowder; DryPowder, Liquid; OtherSolid

Pigment Yellow 65 Basic Attributes

386.36

386.36

229-419-9

DTXSID0052336

2927000090

Characteristics

135.17000

3.88820

DryPowder; DryPowder, Liquid; OtherSolid

1.33

570.1ºC at 760 mmHg

1.6

Pigment Yellow 65 Use and Manufacturing

Methods of Manufacturing

Reaction equation Operating process Weigh 10.3g of color base GP, grind it into a fine powder and add it to a 100ml beaker, and add 13.0ml of 36% hydrochloric acid, while adding 30.0g of crushed ice, and stir. Weigh 4.3g of sodium nitrite to make a 40ml solution, then add 30.0g of crushed ice and stir. Weigh 4.3g sodium nitrite to make 40ml solution, and then add it to the color base GP suspension cooled to 0℃, and ensure that the excess sodium nitrite solution is strongly acidic, carry out the diazotization reaction, and add the sodium nitrite solution. Then, continue the reaction at a temperature of 0-5°C for 1 hour. After the diazotization is over, use urea to destroy the excess nitrous acid; decolorize the activated carbon, filter, and prepare for coupling. Weigh 12.5g of o-methoxyacetanilide, add it to 160ml of water to make a slurry, and add 30% NaOH solution to dissolve it, then adjust the pH to 6.5-7 with glacial acetic acid to make the o-methoxyacetoacetanilide precipitate, add crystals Sodium acetate 20.0g was beaten and stirred. The prepared diazonium salt solution was added to the coupling component suspension at 10-15°C for about 20 minutes, and the end point was controlled by the percolation experiment. After the reaction is completed, it is filtered, washed with distilled water until the filter cake has a pH value of about 7.0, and dried at 80°C to obtain a pigment.

Uses

Used for coloring of ink, paint printing paste, latex, painting pigments, cultural and educational supplies, etc.


Pigments


Building/construction materials not covered elsewhere

Production

1,000,000 - 10,000,000 lb

Construction|Butanamide, 2-[2-(4-methoxy-2-nitrophenyl)diazenyl]-N-(2-methoxyphenyl)-3-oxo-: ACTIVE

Computed Properties

Molecular Weight:386.4
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:7
Exact Mass:386.12263431
Monoisotopic Mass:386.12263431
Topological Polar Surface Area:135
Heavy Atom Count:28
Complexity:593
Undefined Atom Stereocenter Count:1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

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