N-(2-Methylphenyl)-2-methylbenzenamine
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N-(2-Methylphenyl)-2-methylbenzenamine
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CAS No:
617-00-5
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Formula:
C14H15N
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Chemical Name:
N-(2-Methylphenyl)-2-methylbenzenamine
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Synonyms:
4-12-238;Bis(o-tolyl)amine;2,2'-Ditolylamine;2,2'-Iminobis(methylbenzene);N-(2-Methylphenyl)-2-methylbenzenamine;2-Methyl-N-(2-methylphenyl)benzenamine
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CAS No:
N-(2-Methylphenyl)-2-methylbenzenamine Use and Manufacturing
General procedure: A mixture of 2, 4-dimethylaniline (1.12ml, 8.9 mmol), 4-bromodibenzofuran (2g, 8.1 mmol) and sodium tert-butoxide (1.9g, 20 mmol) was suspended in 150ml of toluene. The solution was degassed and saturated with argon. Then added PdCl2(dppf)CH2Cl2 (132mg, 162 mmol). In a protective gas atmosphere and the reaction mixture was heated at boiling overnight. Silica gel with toluene and AlOx mixture was filtered and evaporated in a rotary evaporator. On silica gel with heptane purified oil. Produce 1.9g (82% of theory) of a pale brown oil.Purity 94% (HPLC). The following compounds were prepared analogously:
Computed Properties
Molecular Weight:197.27
XLogP3:4.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:197.120449483
Monoisotopic Mass:197.120449483
Topological Polar Surface Area:12
Heavy Atom Count:15
Complexity:170
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
N-(2-Methylphenyl)-2-methylbenzenamine
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