4-chloro-6-methoxyquinolin-7-ol
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4-chloro-6-methoxyquinolin-7-ol
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CAS No:
205448-31-3
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Formula:
C10H8ClNO2
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Chemical Name:
4-chloro-6-methoxyquinolin-7-ol
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Synonyms:
4-chloro-6-methoxyquinolin-7-ol;4-Chloro-6-Methoxy-7-quinolinol;4-Chloro-7-hydroxy-6-methoxyquinoline;4-Chloro-7-hydroxy-6-Methoxyquinolin;7-Quinolinol, 4-chloro-6-methoxy-;4-Chloro-6-methoxy-7-hydroxyquinoline
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CAS No:
4-chloro-6-methoxyquinolin-7-ol Use and Manufacturing
Compound 114 (16 g, 53.37 mmol) was dissolved in trifluoroacetic acid (100 mL) and MeSOThe 7 - benzyloxy -4 - chloro -6 - methoxy - quinoline (1.675, 5 . 58mmol), glacial acetic acid (10 ml) is added to the 50 ml in the pear-shaped bottle, magnetic stirring under a large amount of white solid. In the system and then to join the hydrogen bromide aqueous solution (40percent, 10 ml), heated to 80 °C reaction 3h. The reaction system is cooled to 45 °C left, poured into 80 ml ethyl ether in stirring, a large number of white solid precipitated, filtered, washed with ethyl ether, dried under vacuum to get white solid. Yield: 80percent.A solution of 7-benzyloxy-4-chloro-6-methoxyquinoline hydrochloride (6.8 g, 20 mmol) in TFA (80 ml) was heated at reflux for 5.5 hours.. Production Example 20:
Computed Properties
Molecular Weight:209.63
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:209.0243562
Monoisotopic Mass:209.0243562
Topological Polar Surface Area:42.4
Heavy Atom Count:14
Complexity:203
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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