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(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID

(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID structure

CAS No:
56453-86-2
Formula:
C9H14O2
Chemical Name:
(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID
Synonyms:
(E)-3-Cyclohexylacrylic acid;(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID;(E)-3-cyclohexylprop-2-enoic acid;3-cyclohexaneacrylic acid;4484-35-9;NSC147133;b-cyclohexylacrylic acid;2-Propenoic acid, 3-cyclohexyl-, (E)-;3-Cyclohexylpropenoic acid;Cyclohexaneacrylic acid, (E)-

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(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID Basic Attributes

Molecular Weight：

154.21

Exact Mass：

154.09900

Characteristics

PSA：

37.3

XLogP3：

2.8

Density：

1.125g/cm3

Melting Point：

58-59 °C

Boiling Point：

283.2°C at 760 mmHg

Flash Point：

189.5ºC

Refractive Index：

1.57

(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID Use and Manufacturing

The hydrolysis of (E)-ethyl 3-cyclohexylacrylate, using the procedure described above, afforded trans-20 (78percent) as colorless needles: mp 46-47 °C (hexane); General procedure: To a solution of 4-acetoxycinnamic acid (41 mg, 0.2 mmol) in THF(1 mL), EDCI (38 mg, 0.2 mmol), DMAP (6 mg, 0.05 mmol), and Et3N (45 L, 0.3 mmol) were added.Then, 16a (27 mg, 0.066 mmol) in THF (1 mL) was added under nitrogen. The solution was stirredat r.t. for 12 h. The organic layer was concentrated in vacuo. The residue was purified by columnchromatography (petroleum ether/EtOAc = 3:1) to give 21 as white solid (24 mg, 45.0%).

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Guide of (2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID

Basic Attributes
Characteristics
Use and Manufacturing
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(2E)-3-CYCLOHEXYLPROP-2-ENOIC ACID

SDS

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