1-(4,5-Dichloro-2-thienyl)ethanone
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1-(4,5-Dichloro-2-thienyl)ethanone
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CAS No:
57681-59-1
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Formula:
C6H4Cl2OS
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Chemical Name:
1-(4,5-Dichloro-2-thienyl)ethanone
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Synonyms:
Ethanone,1-(4,5-dichloro-2-thienyl)-;Ketone,4,5-dichloro-2-thienyl methyl;1-(4,5-Dichloro-2-thienyl)ethanone;2-Acetyl-4,5-dichlorothiophene;4,5-Dichloro-2-acetylthiophene;1-(4,5-Dichlorothiophen-2-yl)ethanone
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CAS No:
1-(4,5-Dichloro-2-thienyl)ethanone Use and Manufacturing
n-Butyl lithium (2.51 g, 39.2 mmol, 24.5 mL) was added dropwise to a stirring solution of diisopropylamine (3.97 g, 39.2 mmol, 5.54 mL) in tetrahydrofuran (5 mL) at -78 °C and stirred for 45 min to generate lithium diisopropylamine (LDA) in situ. 2, 3-Dichlorothiophene (5 g, 32.7 mmol) dissolved in tetrahydrofuran (5 mL) was added dropwise and the mixture was stirred at -78 °C for 30 min. Dimethylformamide (3.41 g, 39.2 mmol, 3.64 mL) dissolved in tetrahydrofuran (5 mL) was added dropwise and the mixture was stirred at -78
1-(4,5-Dichloro-2-thienyl)ethanone
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