bis(4-methylphenyl)diazene
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bis(4-methylphenyl)diazene
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CAS No:
501-60-0
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Formula:
C14H14N2
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Chemical Name:
bis(4-methylphenyl)diazene
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Synonyms:
4,4'-azotoluene;4,4'-Dimethylazobenzene;bis(4-methylphenyl)diazene;4,4'-Azobis(methylbenzene);1,2-Bis(4-methylphenyl)diazene
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CAS No:
Safety Information
P264, P270, P273, P301+P312, P330, P391, P501
H302
|Warning|H302 (100%): Harmful if swallowed [Warning Acute toxicity, oral]|P264, P270, P273, P301+P312, P330, P391, and P501|Aggregated GHS information provided by 38 companies from 1 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.
bis(4-methylphenyl)diazene Use and Manufacturing
General procedure: LiAlH4 (5mmol) was added to a stirred suspension of TiCl4 (1mmol) in diethyl ether. The resulting suspension was stirred at room temperature for 15min. Then a solution in diethyl ether of the corresponding nitro compound (1a, 1mmol) was added slowly to the obtained black reducing suspension under inert nitrogen atmosphere. The reaction was kept stirring at room temperature and monitored by TLC (diethyl ether/petroleum ether 60:40 v/v). After complete conversion of the starting material, the reaction mixture was paper filtered, washed with 1N aqueous NaOH (3×5mL) and once with brine (5mL). The ethereal layers were dried (Na2SO4) and evaporated to dryness under reduced pressure conditions to give the corresponding amine
Computed Properties
Molecular Weight:210.27
XLogP3:4.5
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:210.115698455
Monoisotopic Mass:210.115698455
Topological Polar Surface Area:24.7
Heavy Atom Count:16
Complexity:197
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes
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