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Irgacure 369

Irgacure 369 structure

CAS No:
119313-12-1
Formula:
C23H30N2O2
Chemical Name:
Irgacure 369
Synonyms:
1-Butanone,2-(dimethylamino)-1-[4-(4-morpholinyl)phenyl]-2-(phenylmethyl)-;2-(Dimethylamino)-1-[4-(4-morpholinyl)phenyl]-2-(phenylmethyl)-1-butanone;CGI 369;Irgacure 369;2-Benzyl-2-(dimethylamino)-1-(4-morpholinophenyl)-1-butanone;2-Benzyl-2-dimethylamino-1-(4-morpholinophenyl)butanone;2-Benzyl-2-N,N-dimethylamino-1-(4-morpholinophenyl)-1-butanone;α-Benzyl-α-(dimethylamino)-4-morpholinobutyrophenone;Irg 369;Ciba 369;2-Benzyl-2-(dimethylamino)-1-[4-(4-morpholinyl)phenyl]-1-butanone;IC 369;2-Benzyl-2-(dimethylamino)-1-(4-morpholinophenyl)butanone-1;I 369;Genocure BDMM;JRcure 369;2-Benzyl-2-(dimethylamino)-4′-morpholinobutyrophenone;PI 369;Lancure 369;2-Benzyl-2-(dimethylamino)-4′-mopholinobutyrophenone;Photoinitiator 369;2-(Dimethylamino)-1-(4-morpholinophenyl)-2-benzyl-1-butanone;2-Benzyl-2-dimethylamino-1-(4-morpholinophehyl)-butane-1-one;IHT-PI 910;2-Dimethylamino-2-benzyl-1-[4-(4-morpholino)phenyl]-1-butanone;Irgacure 369E;UV 369;Luna 800;Omnired 369;IGR 369;Omnirad 369E;Omnirad 369;Photoinitiator 910;Omnirad 379;IGM 379;IGM 369;136797-29-0;748160-22-7;1392498-45-1;1393715-98-4;2102600-95-1;2253103-97-6
Categories:
Cosmetic Ingredient > Binding Agent

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Description

Light yellow solid

DryPowder; OtherSolid; PelletsLargeCrystals, Liquid

Irgacure 369 Basic Attributes

Molecular Weight：

366.5

Exact Mass：

366.50

EC Number：

404-360-3

DSSTox ID：

DTXSID5044786

HScode：

29349990

Characteristics

PSA：

32.8

XLogP3：

4.1

Appearance：

DryPowder; OtherSolid; PelletsLargeCrystals, Liquid

Density：

1.094±0.06 g/cm3(Predicted)

Melting Point：

116-119 °C(lit.)

Boiling Point：

528.8±50.0 °C(Predicted)

Flash Point：

>230 °F

Refractive Index：

1.567

Vapor Pressure：

2.87E-11mmHg at 25°C

Safety Information

Packing level：

III

Hazard category：

Transport codes：

UN 3077 9/PG 3

wgk germany：

hazard class code：

50/53

safety instructions：

60-61

RTECS Number：

EL7755000

Marks：

Precautionary statement(s)：

P273-P501

Hazard Statements：

H410

GHS Classification：

|Danger|H360D: May damage the unborn child [Danger Reproductive toxicity]|P201, P202, P273, P281, P308+P313, P391, P405, and P501|Warning|H400 (99.67%): Very toxic to aquatic life [Warning Hazardous to the aquatic environment, acute hazard]|P273, P391, and P501|Aggregated GHS information provided by 304 companies from 9 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.|H360 (51.45%): May damage fertility or the unborn child [Danger Reproductive toxicity]|Aggregated GHS information provided by 311 companies from 14 notifications to the ECHA C&L Inventory. Each notification may be associated with multiple companies.|H318: Causes serious eye damage [Danger Serious eye damage/eye irritation]|P201, P202, P273, P280, P281, P305+P351+P338, P308+P313, P310, P391, P405, and P501

Irgacure 369 Use and Manufacturing

Methods of Manufacturing

To a three-necked flask were placed 800 mL of morpholine, 3 g of copper, 3 ml of EDTA and 1 mol of compound V-1, using a high pressure of 1.1 MPa, a temperature of 180 ° C, and a holding time of 20 hours. LC tracking, the reaction of the compound V-1 is completely the end of the reaction, and then the morpholine is removed under reduced pressure.When the temperature is raised to 120 ° C, the temperature is maintained for 60 min, the solvent is removed, and then the temperature is lowered to 90 ° C. 1000 ml of toluene and 400 ml of water are added for 3 times, and the oil phase is separated and decomposed by vacuum distillation. When the temperature is raised to 120 ° C, the solution is desolvated. After completion, the mixture was cooled to 80 ° C, and 1500 ml of a mixed solvent of toluene and methanol (25percent of toluene) was added for crystallization. After centrifugation and drying, a product of 278.2 g was obtained, the content was 99.4percent, and the yield was 76.0percent.take 2-benzyl-2-dimethylamino-1-P-fluorophenyl-1-butanone dissolve in dichloroethane solution and add morpholine (139.6g, 1 . 6mol) into 1L in four-mouth bottle, heating reflux reaction, TLC or liquid phase chromatographic monitoring reaction, after the reaction is complete, reducing the temperature to room temperature, add 200 ml water washing, stirring 0.5h, layering, the organic phase is separated, and recovering the solvent, by residues 440 ml ethanol is recrystallized to get pale yellow solid 117.2, melting point: 115-116°C, the overall yield is 80percent, purity 99.3percent

Uses

UV solidify ink and coating

Paint additives and coating additives not described by other categories

Paints and coatings

Production

100,000 - 500,000 lb

Manufacturing Info：

Adhesive manufacturing|1-Butanone, 2-(dimethylamino)-1-[4-(4-morpholinyl)phenyl]-2-(phenylmethyl)-: ACTIVE|PMN - indicates a commenced PMN (Pre-Manufacture Notices) substance.

Computed Properties

Molecular Weight:366.5
XLogP3:4.1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:366.230728204
Monoisotopic Mass:366.230728204
Topological Polar Surface Area:32.8
Heavy Atom Count:27
Complexity:461
Undefined Atom Stereocenter Count:1
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Material

Magnesium sulfate heptahydrate

Morpholine

Sodium hydroxide

Sodium benzoate

Potassium carbonate

Acetic acid

Dimethyl sulfoxide

Acetonitrile

Nitrogen

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CAS No.: 119313-12-1

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Guide of Irgacure 369

Description
Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Material
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Irgacure 369

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