 Home > Encyclopedia > N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide]

N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide]

N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide] structure

CAS No:
2379-81-9
Formula:
C42H23N3O6
Chemical Name:
N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide]
Synonyms:
Benzamide,N,N′-(10,15,16,17-tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis-;Indanthrene Olive R;5H-Dinaphtho[2,3-a:2′,3′-i]carbazole-5,10,15,17(16H)-tetrone,6,9-dibenzamido-;5H-Dinaphtho[2,3-a:2′,3′-i]carbazole,benzamide deriv.;N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide];C.I. 69005;Ahcovat Olive R;Ahcovat Olive ARN;Amanthrene Olive R;Atic Vat Olive R;Benzadone Olive R;Calcoloid Olive R;Calcoloid Olive RC;Calcoloid Olive RL;Caledone Olive RP;Caledon Olive R;Carbanthrene Olive R;Cibanone Olive F2R;C.I. Vat Black 27;Fenanthren Olive R;Indanthren Olive R;Mayvat Olive AR;Mikethrene Olive R;Nihonthrene Olive R;Nyanthrene Olive R;Ostanthren Olive R;Palanthrene Olive R;Paradone Olive R;Pernithrene Olive R;Ponsol Olive AR;Ponsol Olive ARD;Romantrene Olive FR;Sandothrene Olive N2R;Solanthrene Olive R;Tinon Olive 2R;Cibanone Olive 2R;Tyrian Olive I-R;Solanthrene Olive F-R;Novatic Olive R;Indanthrene gold orange 3G-FNN;Navinon Olive R;NSC 51543;Novatic Olive Green R;Vat Black 27;Vat Olive R;61356-49-8
Categories:
Dyes and Pigments > Dye

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N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide] Basic Attributes

Molecular Weight：

665.64852

Exact Mass：

665.65

EC Number：

219-169-9

NSC Number：

51543

Characteristics

PSA：

142

XLogP3：

7.52250

Density：

1.537 g/cm3

Boiling Point：

685.54°C (rough estimate)

Refractive Index：

1.831

Safety Information

Precautionary statement(s)：

P261, P272, P280, P302+P352, P321, P333+P313, P363, P501

Hazard Statements：

H317

GHS Classification：

|Warning|H317 (100%): May cause an allergic skin reaction [Warning Sensitization, Skin]|P261, P272, P280, P302+P352, P321, P333+P313, P363, and P501|Aggregated GHS information provided by 24 companies from 2 notifications to the ECHA C&L Inventory.

N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide] Use and Manufacturing

Methods of Manufacturing

Using 1-aminoanthraquinone and 1-chloroanthraquinone as raw materials, the two are first condensed in the presence of copper powder, then nitrated and reduced, benzoylated with benzoyl chloride, and then closed and oxidized to obtain the product . After filtering, drying and crushing, the finished product is obtained. . 1 part of 1-chloroanthraquinone, 1.047 parts of 1-aminoanthraquinone, 36.65 parts of nitrobenzene, 1.016 parts of sodium carbonate, 2.5g of copper sulfate (industrial product) were subjected to condensation reaction at 205-210℃ for 9h to obtain " Amine" (I). After nitrifying 3.99g boric acid (100%), 149.6g sulfuric acid (100%), 24.6g industrial mixed acid and 18.79g "imine" (I) (100%) at 20-25℃, use 15.38g sodium sulfide (100%) %) is reduced to (II). 23.01 parts of o-dichlorobenzene, 2.75 parts of benzoyl chloride, and 1 part of (II) are closed at 150°C, oxidized with potassium chlorate (or sodium chlorate), filtered, and washed with water to neutrality to obtain 10g of dye. This product can also be condensed with 1-benzylamino-4-chloroanthraquinone and 1-amino-4-benzylaminoanthraquinone in the presence of copper, and the product can be obtained by ring closure.

Uses

Used for dyeing cellulose fibers

Manufacturing Info：

Benzamide, N,N'-(10,15,16,17-tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2',3'-i]carbazole-6,9-diyl)bis-: ACTIVE

Computed Properties

Molecular Weight:665.6
XLogP3:8.1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:665.15868546
Monoisotopic Mass:665.15868546
Topological Polar Surface Area:142
Heavy Atom Count:51
Complexity:1340
Covalently-Bonded Unit Count:1
Compound Is Canonicalized:Yes

Material

Sulfuric acid

Copper sulfate

1,2-Dichlorobenzene

Latest News on N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide]

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Guide of N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide]

Basic Attributes
Characteristics
Safety Information
Use and Manufacturing
Computed Properties
Material
Latest News
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N,N′-(10,15,16,17-Tetrahydro-5,10,15,17-tetraoxo-5H-dinaphtho[2,3-a:2′,3′-i]carbazole-6,9-diyl)bis[benzamide]

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